CN105698977A - Application of WTe2 monocrystalline as low-temperature pressure transducer material - Google Patents

Application of WTe2 monocrystalline as low-temperature pressure transducer material Download PDF

Info

Publication number
CN105698977A
CN105698977A CN201610163120.2A CN201610163120A CN105698977A CN 105698977 A CN105698977 A CN 105698977A CN 201610163120 A CN201610163120 A CN 201610163120A CN 105698977 A CN105698977 A CN 105698977A
Authority
CN
China
Prior art keywords
monocrystalline
wte
temperature
low
resistance value
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610163120.2A
Other languages
Chinese (zh)
Inventor
李世燕
蔡鹏林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fudan University
Original Assignee
Fudan University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fudan University filed Critical Fudan University
Priority to CN201610163120.2A priority Critical patent/CN105698977A/en
Publication of CN105698977A publication Critical patent/CN105698977A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L1/00Measuring force or stress, in general
    • G01L1/12Measuring force or stress, in general by measuring variations in the magnetic properties of materials resulting from the application of stress
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L9/00Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
    • G01L9/16Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means by making use of variations in the magnetic properties of material resulting from the application of stress

Landscapes

  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Measuring Fluid Pressure (AREA)

Abstract

The invention, which belongs to the technical field of the low-temperature pressure transducer, particularly provides an application of a WTe2 monocrystalline as a low-temperature pressure transducer material. According to the invention, on the basis of the characteristic of the great difference between reluctances of the WTe2 monocrystalline under different pressures at a low temperature, the WTe2 monocrystalline can be used as a pressure transducer with high sensitivity at a low temperature. The experiment demonstrates that the reluctance values of the WTe2 monocrystalline material under different pressures are different from each other obviously. When the temperature is 0.3K and the magnetic field is 14.5T, the reluctance value can reach 125000% under the pressure of 0 kbar. The reluctance value is in an obvious downtrend with increase of the pressure; and when the pressure reaches 23.6 kbar, the reluctance value is only 7470%.

Description

WTe2Monocrystalline is as the application of low-temperature pressure sensor material
Technical field
The invention belongs to low-temperature pressure sensor technical field, be specifically related to WTe2Monocrystalline is as the application of new type low temperature pressure transducer material。
Background technology
Pressure transducer is the sensor that pressure is converted to signal of telecommunication output。It is a kind of means very common in industry and scientific research that system applies at present pressure。And be one significantly invent for the pressure size of applying can be calibrated exactly。Pressure transducer is widely used in various industry automatic control environment by industrial practice, has related to penetrating among numerous related application industry。And in scientific research, the accurate force value that must calibrate in pressure environment can have important impact for the pressure effect of research system。Current many instruments are to adopt plumbous (Pb) or stannum (Sn) simple substance as superconducting coil, have the feature of relative significant change to demarcate the force value of system according to its superconducting transition temperature at various pressures。But the parameter attribute that under searching different pressures, rate of change becomes apparent from can more precisely calibrate pressure。
Summary of the invention
It is an object of the invention to overcome prior art not enough, it is proposed to a kind of WTe2Monocrystalline is as the application of low-temperature pressure sensor material, and this material can more precisely calibrate force value at various pressures。
The WTe that the present invention proposes2Monocrystalline, as the application of low-temperature pressure sensor material, concretely comprises the following steps:
(1) first, by WTe2Electrode made by monocrystalline so that electric current flows along tungsten chain direction (a direction);
(2) then, the WTe of electrode will be carried out2Monocrystalline is inserted in below 5K low temperature environment;
(3) then, apply high-intensity magnetic field along single crystalline vertical in tungsten tellurium layer direction (c direction), obtain the magnetic resistance value of this monocrystalline;
(4) repeat step (1), (2), (3) at various pressures, demarcate the magnetic resistance value of this sample under different pressures;
(5) last, utilize WTe2Monocrystalline magnetic resistance value at various pressures has the feature of significant difference, applies the magnetic field of some strength, with the WTe demarcated2Monocrystalline is as pressure transducer material more accurate under low temperature。
Present invention additionally comprises Te2Monocrystalline is as the low-temperature pressure sensor of sensing material。
The present invention utilizes WTe2Monocrystalline magnetic resistance value at various pressures has the feature of significant difference, substantially increases the accurate resolution of pressure, can as good pressure transducer material。Experiments show that, at low temperatures, this material magnetic resistance value at various pressures has the difference of highly significant。When temperature be 0.3K magnetic field is 14.5T, when 0kbar, magnetic resistance value has reached 125000%。But being as the increase of pressure, magnetic resistance has a significantly downward trend, and when pressure reaches 23.6kbar, magnetic resistance value is only 7470%。And when temperature is in 0.3K, force value from 0kbar change to 23.6kbar time, traditional pressure resolved way (utilizes stannum (Sn) simple substance as superconducting coil, have the feature of relative significant change to demarcate the force value of system according to its superconducting transition temperature at various pressures) have 28% decline, and the WTe of the present invention2Monocrystalline magnetic resistance value at various pressures has the decline of 94%, and the parameter comparing traditional nominal pressure change becomes apparent from significant decline, it is possible to be used for more accurately calibrating the different pressures value under low temperature。
Accompanying drawing explanation
Fig. 1 implements the WTe in step process in embodiment 1-22Monocrystalline pattern picture。
Fig. 2 implements the WTe in step process in embodiment 1-22Mono-crystalline structures figure。
Fig. 3 implements the WTe in step process in embodiment 1-22Single crystal X-ray diffraction figure。
Fig. 4 is the embodiment 1-2 WTe when 0.3K finally obtained afterwards2Monocrystalline is magnetic resistance value figure at various pressures。
Fig. 5 is the embodiment 1-2 WTe when 0.3K finally obtained afterwards2Monocrystalline is magnetic resistance change rate figure at various pressures。
Detailed description of the invention
Below in conjunction with drawings and Examples, technical solution of the present invention is described further。
Embodiment 1, a kind of new type low temperature pressure transducer material WTe2Monocrystalline and application thereof。
1, first, a piece of 2.0*0.7*0.02mm is selected3Size WTe2Monocrystalline, by WTe2Electrode carried out by monocrystalline so that electric current flows along a direction, and recording its room temperature resistivity is 355 μ Ω * cm。
2, being lowered the temperature from room temperature by sample, resistivity when obtaining 2k is 1.93 μ Ω * cm。
3, temperature is controlled at 0.3K, apply the high-intensity magnetic field along monocrystalline c direction, it is possible to obtain the magnetic resistance value of this monocrystalline。
4, at various pressures repetitive process (1), (2), (3), it is possible to demarcate the magnetic resistance value of this sample under different pressures。
5 finally, due to WTe2Monocrystalline magnetic resistance value at various pressures has significant difference, it is possible to the WTe demarcated2Monocrystalline is as pressure transducer material more accurate under low temperature。
Embodiment 2, a kind of new type low temperature pressure transducer material WTe2Monocrystalline and application thereof。
1, a piece of 2.15*0.55*0.02mm is first selected3Size WTe2Monocrystalline, by WTe2Monocrystalline is carried out electrode and electric current is flowed along a direction, and recording its room temperature resistivity is 396 μ Ω * cm。
2, being lowered the temperature from room temperature by sample, resistivity when obtaining 2k is 2.31 μ Ω * cm。
3, temperature is controlled at 0.3K, apply the high-intensity magnetic field along monocrystalline c direction, it is possible to obtain the magnetic resistance value of this monocrystalline。
4, at various pressures repetitive process (1), (2), (3), it is possible to demarcate the magnetic resistance value of this sample under different pressures。
5 finally, due to WTe2Monocrystalline magnetic resistance value at various pressures has significant difference, it is possible to the WTe demarcated2Monocrystalline is as pressure transducer material more accurate under low temperature。
Embodiment 3, a kind of new type low temperature pressure transducer material WTe2Monocrystalline and application thereof。
1, a piece of 2.0*0.69*0.02mm is first selected3Size WTe2Monocrystalline, by WTe2Monocrystalline is carried out electrode and electric current is flowed along a direction, and recording its room temperature resistivity is 403 μ Ω * cm。
2, being lowered the temperature from room temperature by sample, resistivity when obtaining 2k is 1.95 μ Ω * cm。
3, temperature is controlled at 0.3K, apply the high-intensity magnetic field along monocrystalline c direction, it is possible to obtain the magnetic resistance value of this monocrystalline。
4, at various pressures repetitive process (1), (2), (3), it is possible to demarcate the magnetic resistance value of this sample under different pressures。
5 finally, due to WTe2Monocrystalline magnetic resistance value at various pressures has significant difference, it is possible to the WTe demarcated2Monocrystalline is as pressure transducer material more accurate under low temperature。
Fig. 1 is WTe2Monocrystalline pattern photo。It will be clear that WTe2Monocrystalline has obviously along the striped in a direction。Fig. 2 is WTe2Monocrystalline structure cell schematic diagram, has obvious zigzag shape along W chain direction。Fig. 3 is WTe2The X-ray diffractogram of monocrystalline, lattice paprmeter c=14.054 angstrom obtained。
The present embodiment is by by WTe2Monocrystalline is carried out electrode and is made electric current be placed in low temperature environment along the flowing of a direction, applies the high-intensity magnetic field along monocrystalline c direction at various pressures, it is possible to obtain the magnetic resistance value of this monocrystalline, as shown in Figure 4。When 14.5T, the magnetic resistance value (numerical value of smooth back end) under each pressure is analyzed respectively, it is possible to finding along with the change of pressure, magnetic resistance (0.3K, 14.5T) has the change obviously declined, and therefore, it can with the WTe demarcated2Monocrystalline is as pressure transducer material more accurate under low temperature。

Claims (2)

1.WTe2Monocrystalline is as the application of low-temperature pressure sensor material, it is characterised in that concretely comprise the following steps:
(1) first, by WTe2Electrode made by monocrystalline so that electric current connects direction flowing along tungsten;
(2) then, the WTe of electrode will be carried out2Monocrystalline is inserted in below 5K low temperature environment;
(3) then, apply high-intensity magnetic field along single crystalline vertical in tungsten tellurium layer direction, obtain the magnetic resistance value of this monocrystalline;
(4) repeat step (1), step (2), step (3) at various pressures, demarcate the magnetic resistance value of this sample under different pressures;
(5) last, utilize WTe2Monocrystalline magnetic resistance value at various pressures has the feature of significant difference, applies the magnetic field of some strength, with the WTe demarcated2Monocrystalline is as pressure transducer material more accurate under low temperature。
2. one kind by WTe2Monocrystalline is as the low-temperature pressure sensor of sensing material。
CN201610163120.2A 2016-03-19 2016-03-19 Application of WTe2 monocrystalline as low-temperature pressure transducer material Pending CN105698977A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610163120.2A CN105698977A (en) 2016-03-19 2016-03-19 Application of WTe2 monocrystalline as low-temperature pressure transducer material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610163120.2A CN105698977A (en) 2016-03-19 2016-03-19 Application of WTe2 monocrystalline as low-temperature pressure transducer material

Publications (1)

Publication Number Publication Date
CN105698977A true CN105698977A (en) 2016-06-22

Family

ID=56231549

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610163120.2A Pending CN105698977A (en) 2016-03-19 2016-03-19 Application of WTe2 monocrystalline as low-temperature pressure transducer material

Country Status (1)

Country Link
CN (1) CN105698977A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004001805A2 (en) * 2002-06-21 2003-12-31 California Institute Of Technology Sensors based on giant planar hall effect in dilute magnetic semiconductors
CN1725455A (en) * 2004-07-19 2006-01-25 精工爱普生株式会社 Method for fabricating a semiconductor element from a dispersion of semiconductor particles
CN102084513A (en) * 2008-07-08 2011-06-01 住友化学株式会社 Photoelectric conversion element

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004001805A2 (en) * 2002-06-21 2003-12-31 California Institute Of Technology Sensors based on giant planar hall effect in dilute magnetic semiconductors
CN1725455A (en) * 2004-07-19 2006-01-25 精工爱普生株式会社 Method for fabricating a semiconductor element from a dispersion of semiconductor particles
CN102084513A (en) * 2008-07-08 2011-06-01 住友化学株式会社 Photoelectric conversion element

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
MAZHAR N. ALI: "Large, non-saturating magnetoresistance in WTe2", 《NATURE》 *
P.L.CAI: "Drastic pressure e_ect on the extremely large magnetoresistance in WTe2: quantum oscillation study", 《PHYSICAL REVIEW LETTERS》 *

Similar Documents

Publication Publication Date Title
EP2612122B1 (en) Method and apparatus for calibrating a thermometer in situ
EP3551981B1 (en) Method for the in-situ calibration of a thermometer
US20140130591A1 (en) Methods and Apparatus for Determining Downhole Parameters
DE3628017A1 (en) THERMAL FLOW SENSOR
DE102007053859A1 (en) Pressure-measuring device
EP2921833B1 (en) Thermoanalytical sensor and method for its production
US9766173B2 (en) Multimodal sensor including a tensiometer, method of use and fabrication
CN104345084B (en) PH sensors with the bonding agent being arranged in patterns
JP2024019227A (en) Systems and methods for process condition measurement wafer assembly
CN105492718A (en) Downhole cooling with electrocaloric effect
US10174603B2 (en) Downhole visualisation method
CN105698977A (en) Application of WTe2 monocrystalline as low-temperature pressure transducer material
CN110196115B (en) Method for measuring temperature by using magnetic tunnel junction magnetoresistance
KR102633304B1 (en) Hall Sensor of using Anomalous Hall Effect and Method of manufacturing the same
JP4528943B2 (en) Capacitance temperature sensor and temperature measuring device
CN105047814A (en) Si-based magnetic sensing device with low magnetic field and giant magnetoresistance, preparation method and performance testing method
CN104345083B (en) There are the pH sensors of the substrate or binder course that are configured to maintain ISFET tube core piezoresistances
DE102016103563A1 (en) Method for detecting a substance contained in a gaseous medium, computer program, evaluation unit and sensor device
RU46857U1 (en) DEVICE FOR THERMOMAGNETIC MEASUREMENTS UNDER PRESSURE
EP3325958A1 (en) Sensor element for a chemical sensor and chemical sensor
EP3012604B1 (en) Sensor for the detection of infrared radiation and method for operating the sensor
DE102016210300A1 (en) Microelectromechanical bolometer and method for detecting an ambient temperature
RU2380206C2 (en) Method for manufacturing of nuclear reactor fuel element
CN203271722U (en) Storage type axial tension recording device of under-pit oil pipe
DE102016010974A1 (en) Material conversion arrangement and method

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20160622